5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose

Base Information

Chemical Name:5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose
CAS No.:1162686-87-4
Molecular Formula:C₃₄H₃₇NO₆
Molecular Weight:555.671
Hs Code.:

Synonyms:5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose

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Chemical Property of 5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose

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Technology Process of 5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose

There total 1 articles about 5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5-O-benzyl-7-benzylamino-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-ido-and-α-L-gluco-nona-1,8-dien-3-ulofuranose

: 501-53-1,94274-21-2
benzyl chloroformate

: 1162686-87-4
5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 2.5h;
DOI:10.1002/ejoc.200801232

Reference yield: 79.0%

: 1162686-87-4
5-O-benzyl-7-[(benzyl)(benzyloxycarbonyl)amino]-1,2,7,8,9-pentadeoxy-3,4-O-isopropylidene-β-D-talo-nona-1,8-dien-3-ulofuranose

: 1162686-88-5
(1S,4R,5S,6S,7S)-6-benzyloxy-4-[(benzyl)(benzyloxycarbonyl)amino]-1,7-isopropylidenedioxy-8-oxabicyclo[3.2.1]oct-2-ene

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 100 ℃; for 2h; Microwave irradiation; Inert atmosphere;
DOI:10.1002/ejoc.200801232