HEXABENZILISOVYURTSITAN

Base Information

• Chemical Name: HEXABENZILISOVYURTSITAN
• CAS No.: 124782-15-6
• Molecular Formula: C₄₈H₄₈N₆
• Molecular Weight: 708.949
• Mol file: 124782-15-6.mol

Synonyms:2,4,6,8,10,12-hexabenzyl-2,4,5,8,10,12-hexaazatetracyclo[5.5.0.0^3,11.0^5,9]dodecane

Chemical Property of HEXABENZILISOVYURTSITAN

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HEXABENZILISOVYURTSITAN

There total 9 articles about HEXABENZILISOVYURTSITAN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Glyoxal (131543-46-9,107-22-2) + benzylamine (100-46-9) → 2,4,6,8,10,12-hexabenzyl-2,4,5,8,10,12-hexaazatetracyclo[5.5.0.03,11.05,9]dodecane (124782-15-6)

Guidance literature:

With Ni_0.35Cu_0.25Zn_0.4Fe₂O₄; In water; acetonitrile; for 0.0833333h; Solvent; Time; Catalytic behavior; Sonication; Green chemistry;

DOI:10.1134/S0022476618070296

Reference yield: 90.0%

Glyoxal (131543-46-9,107-22-2) + benzylamine (100-46-9) → 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazaisowurtzitane(HBIW) + 2,4,6,8,10,12-hexabenzyl-2,4,5,8,10,12-hexaazatetracyclo[5.5.0.03,11.05,9]dodecane (124782-15-6)

Guidance literature:

With formic acid; In water; acetonitrile;

Reference yield: 73.0%

2,3-dihydroxy-1,4-dioxane (4845-50-5) + benzylamine (100-46-9) → 2,4,6,8,10,12-hexabenzyl-2,4,5,8,10,12-hexaazatetracyclo[5.5.0.03,11.05,9]dodecane (124782-15-6)

Guidance literature:

formic acid; In water; acetonitrile; at 25 ℃; for 18h;

DOI:10.1021/jo00292a015

upstream raw materials:

2,3-dihydroxy-1,4-dioxane

benzylamine

Glyoxal

N,N'-Dibenzyl-1,2-ethanediimine

Downstream raw materials:

1,3-dibenzylimidazolidine-2,4,5-trione

2,6,8,12-tetraacetyl-4,10-dibenzyl-2,4,5,8,10,12-hexaazatetracyclo[5.5.0.0^3,11.0^5,9]dodecane

1-benzylimidazole

1,3-dibenzyl-1,3-diazolidine

Refernces

• 1、 Il'yasov, Sergey G,Chikina, Maya V.. "Novel approach for the synthesis of hexaazaisowurtzitane derivatives". . p. 1931 - 1932. Retrieved 2013.
• 2、 Lin, Gialih,Tsai, Hou-Jen,Tsai, Yi-Hon. "Cage amines as the stopper inhibitors of cholinesterases". . p. 2887 - 2890. Retrieved 2003.
• 3、 Qian, Hua,Lv, Chunxu,Ye, Zhiwen. "Synthesis of CL-20 by clean nitrating agent dinitrogen pentoxide". body text. p. 434 - 439. Retrieved 2009/08/08.