methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

Base Information

Chemical Name:methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate
CAS No.:1247827-83-3
Molecular Formula:C₂₅H₁₈ClNO₃
Molecular Weight:415.876
Hs Code.:

Synonyms:methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

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Chemical Property of methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

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Technology Process of methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

There total 4 articles about methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1183609-32-6
methyl 2-{[(3-bromophenyl)carbonyl]amino}-5-chlorobenzoate

: 13922-41-3
1-Naphthylboronic acid

: 1247827-83-3
methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; water; toluene; for 7.5h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2017.11.016

Reference yield: 79.0%

: 1247827-83-3
methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

Guidance literature:

Reference yield:

: 585-76-2
m-bromobenzoic acid

: 1247827-83-3
methyl 5-chloro-2-({[3-(naphthalen-1-yl)phenyl]carbonyl}amino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 2 h / 20 °C

1.2: 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; toluene; water / 7.5 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; sodium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; water; toluene; 2.1: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2017.11.016