Ca{C(SiHMe₂)₃}₂TMEDA

Base Information

• Chemical Name: Ca{C(SiHMe₂)₃}₂TMEDA
• CAS No.: 1426156-46-8
• Molecular Formula: C₂₀H₅₈CaN₂Si₆
• Molecular Weight: 535.285

Synonyms:Ca{C(SiHMe₂)₃}₂TMEDA

Chemical Property of Ca{C(SiHMe₂)₃}₂TMEDA

Chemical Property:

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Technology Process of Ca{C(SiHMe₂)₃}₂TMEDA

There total 1 articles about Ca{C(SiHMe₂)₃}₂TMEDA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N,N,N,-tetramethylethylenediamine (110-18-9) + Ca{tris(dimethylsilyl)methyl}2(tetrahydrofuran)2 (1192824-26-2) → tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + Ca{C(SiHMe2)3}2TMEDA (1426156-46-8)

Guidance literature:

In benzene-d6; for 0.0833333h; Inert atmosphere;

DOI:10.1021/om3010299

Reference yield: 70.3%

Ca{C(SiHMe2)3}2TMEDA (1426156-46-8) + tris(pentafluorophenyl)borate (1109-15-5) → (Me2SiC(SiHMe2)2)2 (225096-56-0) + Ca{κ3-H,o-F,o-F-hydridotris(perfluorophenyl)borato}2(TMEDA) (1426156-50-4)

Guidance literature:

In benzene; at 20 ℃; Inert atmosphere;

DOI:10.1021/om3010299

Reference yield: 65.7%

Ca{C(SiHMe2)3}2TMEDA (1426156-46-8) + tris(pentafluorophenyl)borate (1109-15-5) → (Me2SiC(SiHMe2)2)2 (225096-56-0) + Ca{tris(dimethylsilyl)methyl}{κ3-H,o-F,o-F-hydridotris(perfluorophenyl)borato}(TMEDA) (1426156-48-0)

Guidance literature:

In benzene; at 20 ℃; for 0.75h; Inert atmosphere;

DOI:10.1021/om3010299

upstream raw materials:

N,N,N,N,-tetramethylethylenediamine

Ca{tris(dimethylsilyl)methyl}₂(tetrahydrofuran)₂

Downstream raw materials:

(Me₂SiC(SiHMe₂)2)2

Ca{tris(dimethylsilyl)methyl}{κ³-H,o-F,o-F-hydridotris(perfluorophenyl)borato}(TMEDA)

Ca{κ³-H,o-F,o-F-hydridotris(perfluorophenyl)borato}₂(TMEDA)

trimethylsilan

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