di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]

Base Information

Chemical Name:di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]
CAS No.:85931-23-3
Molecular Formula:C₁₄H₂₈Cl₂Pd₂S₂
Molecular Weight:544.254
Hs Code.:

Synonyms:di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]

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Chemical Property of di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]

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Technology Process of di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]

There total 2 articles about di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 73061-68-4
dichloro(2,2-dimethylbut-3-en-1-yl methyl sulphide)palladium(II)

: 85931-23-3
di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]

: 85931-27-7
(CCHOC(CH₃)2CH₂S(CH₃)PdClS(CH₃)CH₂C(CH₃)2CH₂CH(OCH₃)2)

: 7440-05-3
palladium

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; byproducts: CH2CH(OMe)2, CH2CHO, CHCH2; a suspn. of Pd-compd. in MeOH-CH2Cl2 contg. ethyldi-isopropylamine (1 equiv) was wtirred was stirred for 4 d at ambient temp., during which time Pd pptd.; further by-products;; the filtrate was subjected to t.l.c. (methanol-CH2Cl2); detected by NMR-expt.; elem. anal.;;

Reference yield:

: 85931-24-4
(CCH₂OCH₃C(CH₃)2CH₂S(CH₃)PdCl)2

: 73061-68-4
dichloro(2,2-dimethylbut-3-en-1-yl methyl sulphide)palladium(II)

: 85931-23-3
di-μ-chloro-bis[(1,2,2-trimethyl-3-methylthiopropyl-C(1),S)palladium(II)]

: 85931-25-5
(CCHOC(CH₃)2CH₂S(CH₃)PdCl)2

: 85931-26-6
(CCO₂CH₃C(CH₃)2CH₂S(CH₃)PdCl)2

: 7440-05-3
palladium

Guidance literature:: In chloroform-d1; byproducts: PdCHCH3; at ambient temp. for 4 d in CDCl3; further by-products; further products;; preparative t.l.c. (methanol-CH2Cl2); monitoring by NHR-expt.; elem. anal.;;