benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

Base Information

Chemical Name:benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside
CAS No.:81102-12-7
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

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Chemical Property of benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

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Technology Process of benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

There total 10 articles about benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: benzyl 4-azido-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

: 81102-12-7
benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; Ambient temperature;
DOI:10.1016/0008-6215(91)89015-8

Reference yield:

: benzyl 4-azido-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threopentopyranoside

: 81102-12-7
((2S,3S,5S)-5-Amino-2-benzyloxy-tetrahydro-pyran-3-yl)-carbamic acid benzyl ester

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; Ambient temperature;
DOI:10.1016/0008-6215(91)89015-8

Reference yield:

: Methanesulfonic acid (3S,5R)-5-amino-6-benzyloxy-tetrahydro-pyran-3-yl ester

: 81102-12-7
benzyl 4-amino-2-(benzyloxycarbonyl)amino-2,3,4-trideoxy-β-DL-threo-pentopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaHCO₃ / dioxane; H₂O / 1 h / Ambient temperature

2: 40 percent / NaN₃, HMPA / 8 h / 80 °C

3: H₂, NEt₃ / 10percent Pd-C / dioxane / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; hydrogen; sodium hydrogencarbonate; triethylamine; palladium on activated charcoal; In 1,4-dioxane; water;
DOI:10.1016/0008-6215(91)89015-8