Os(CO)4(Re(CO)5)2

Base Information

Chemical Name:Os(CO)4(Re(CO)5)2
CAS No.:33153-70-7
Molecular Formula:C₁₄O₁₄OsRe₂
Molecular Weight:954.76
Hs Code.:

Synonyms:Os(CO)4(Re(CO)5)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os(CO)4(Re(CO)5)2

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Technology Process of Os(CO)4(Re(CO)5)2

There total 1 articles about Os(CO)4(Re(CO)5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 22372-70-9,18972-42-4
H₂Os(CO)4

: 75149-83-6
ethylpentacarbonylrhenium

: 33153-70-7
Os(CO)4(Re(CO)5)2

: 123-38-6
propionaldehyde

Guidance literature:: With carbon monoxide; In acetonitrile; EtRe(CO)5, H2Os(CO)4 (2:1 ratio) and MeCN were distilled in a reaction bulb, heated to 60°C overnight, solvent was removed, residue taken up in CH2Cl2, frozen, degassed, CO (2 atm) was admitted, reaction stirred in the dark at room temp. for 2 d; carbonyl complex was isolated via preparative layer chromy. and identified by its known IR spectrum;