C₁₈H₂₆ClNO₅

Base Information

Chemical Name:C₁₈H₂₆ClNO₅
CAS No.:951327-56-3
Molecular Formula:C₁₈H₂₆ClNO₅
Molecular Weight:371.861
Hs Code.:

C<sub>18</sub>H<sub>26</sub>ClNO<sub>5</sub>

Synonyms:C₁₈H₂₆ClNO₅

Suppliers and Price of C₁₈H₂₆ClNO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₈H₂₆ClNO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₈H₂₆ClNO₅

There total 9 articles about C₁₈H₂₆ClNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₄ClNO₅

: 951327-56-3
C₁₈H₂₆ClNO₅

Guidance literature:: With sodium cyanoborohydride; In methanol; at 18 ℃; for 1h;
DOI:10.1021/ol071344y

Reference yield:

: 951327-39-2
C₁₈H₂₅ClO₇

: 951327-56-3
C₁₈H₂₆ClNO₅

Guidance literature:: Multi-step reaction with 7 steps

1: 66 percent / triiodoimidazole; imidazole; PPh₃ / toluene / 5 h / Heating

2: 84 percent / n-Bu₃SnH; Et₃B; O₂ / toluene; hexane / 2 h / 18 °C

3: 98 percent / DDQ / CH₂Cl₂; H₂O / 20 h / 18 °C

4: 75 percent / diphenylphosphoryl azide; DEAD; PPh₃ / CH₂Cl₂ / 18 h / 18 °C

5: 98 percent / PPh₃; H₂O / tetrahydrofuran / 20 h / 65 °C

6: benzene / 16 h / Heating

7: sodium cyanoborohydride / methanol / 1 h / 18 °C

With 1H-imidazole; triethyl borane; tri-iodoimidazole; diphenylphosphoranyl azide; water; oxygen; tri-n-butyl-tin hydride; sodium cyanoborohydride; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene; benzene; 4: Mitsunobu reaction / 5: Staudinger reaction;
DOI:10.1021/ol071344y

Reference yield:

: 951327-37-0
C₁₈H₂₃ClO₇

: 951327-56-3
C₁₈H₂₆ClNO₅

Guidance literature:: Multi-step reaction with 8 steps

1: 60 percent / DIBAL-H / toluene / 7.5 h / -30 °C

2: 66 percent / triiodoimidazole; imidazole; PPh₃ / toluene / 5 h / Heating

3: 84 percent / n-Bu₃SnH; Et₃B; O₂ / toluene; hexane / 2 h / 18 °C

4: 98 percent / DDQ / CH₂Cl₂; H₂O / 20 h / 18 °C

5: 75 percent / diphenylphosphoryl azide; DEAD; PPh₃ / CH₂Cl₂ / 18 h / 18 °C

6: 98 percent / PPh₃; H₂O / tetrahydrofuran / 20 h / 65 °C

7: benzene / 16 h / Heating

8: sodium cyanoborohydride / methanol / 1 h / 18 °C

With 1H-imidazole; triethyl borane; tri-iodoimidazole; diphenylphosphoranyl azide; water; oxygen; tri-n-butyl-tin hydride; diisobutylaluminium hydride; sodium cyanoborohydride; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene; benzene; 5: Mitsunobu reaction / 6: Staudinger reaction;
DOI:10.1021/ol071344y