C₃₈H₃₆B₂N₂O₈

Base Information

• Chemical Name: C₃₈H₃₆B₂N₂O₈
• CAS No.: 1365541-10-1
• Molecular Formula: C₃₈H₃₆B₂N₂O₈
• Molecular Weight: 670.334
• Mol file: 1365541-10-1.mol

Synonyms:C₃₈H₃₆B₂N₂O₈

Chemical Property of C₃₈H₃₆B₂N₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₃₆B₂N₂O₈

There total 2 articles about C₃₈H₃₆B₂N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N,N'-bis(4-iodophenyl)naphthalene-1,4,5,8-tetracarboxylic diimide (895716-36-6) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → C38H36B2N2O8 (1365541-10-1)

Guidance literature:

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine; In toluene; at 100 ℃; for 12h; Inert atmosphere;

DOI:10.1002/anie.201107070

Reference yield:

1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) → C38H36B2N2O8 (1365541-10-1)

Guidance literature:

Multi-step reaction with 2 steps

1: propionic acid / 18 h / 140 °C / Inert atmosphere

2: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine / toluene / 12 h / 100 °C / Inert atmosphere

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); propionic acid; N-ethyl-N,N-diisopropylamine; In toluene;

DOI:10.1002/anie.201107070

Reference yield: 70.0%

C38H36B2N2O8 (1365541-10-1) → C26H16B2N2O8 (1339900-41-2)

Guidance literature:

C₃₈H₃₆B₂N₂O₈; With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 18h;

DOI:10.1002/anie.201107070

upstream raw materials:

N,N'-bis(4-iodophenyl)naphthalene-1,4,5,8-tetracarboxylic diimide

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

1,4,5,8-naphthalenetetracarboxylic dianhydride

Downstream raw materials:

C₂₆H₁₆B₂N₂O₈