2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano⁽¹²⁾]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane

Base Information

• Chemical Name: 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano⁽¹²⁾]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane
• CAS No.: 1537192-12-3
• Molecular Formula: C₁₆H₃₀B₂₀O₄P₂
• Molecular Weight: 564.579

Synonyms:2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano⁽¹²⁾]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane

Chemical Property of 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano⁽¹²⁾]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane

Chemical Property:

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Technology Process of 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano⁽¹²⁾]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane

There total 3 articles about 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano⁽¹²⁾]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dilithium 1,2-Dicarba-closo-dodecaborane-1,2-diolate + Dichlorophenylphosphine (644-97-3) → 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano(12)]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane (1537192-12-3)

Guidance literature:

In ⁽²⁾H₈-toluene; at -30 - 20 ℃; for 2h;

DOI:10.1002/ejic.201301219

Reference yield: 90.0%

dilithium 1,2-Dicarba-closo-dodecaborane-1,2-diolate + Dichlorophenylphosphine (644-97-3) → 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano(12)]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane (1537192-12-3) + C18H40B30O6P2

Guidance literature:

In ⁽²⁾H₈-toluene; at -30 - 20 ℃; for 2h;

DOI:10.1002/ejic.201301219

Reference yield: 80.0%

dilithium 1,2-dicarba-closo-dodecaborane-1,2-diolate + Dichlorophenylphosphine (644-97-3) → 2,7-diphenyl-4,5,9,10-bis[1,2-dicarba-closododecaborano(12)]-2,7-diphospha-1,3,6,8-tetraoxacyclodecane (1537192-12-3) + C14H20B10Cl2O2P2 (1537192-45-2)

Guidance literature:

dilithium 1,2-dicarba-closo-dodecaborane-1,2-diolate; Dichlorophenylphosphine; In ⁽²⁾H₈-toluene; at 20 ℃; for 24h;

In dichloromethane-d2; ⁽²⁾H₈-toluene;

DOI:10.1002/ejic.201301219

upstream raw materials:

Dichlorophenylphosphine

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