methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

Base Information

Chemical Name:methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate
CAS No.:80482-95-7
Molecular Formula:C₁₀H₁₆O₄
Molecular Weight:200.235
Hs Code.:

Synonyms:methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

Chemical Property:

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Technology Process of methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

There total 1 articles about methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2914-23-0
barium methoxide

: 80482-92-4
ethyl 1-benzoyloxy-cis-2-hydroxy-trans-3-methyl-5-methylenecyclohexanecarboxylate

: 80482-95-7
methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

Guidance literature:: In methanol; for 72h;
DOI:10.1021/ja00368a015

Reference yield: 90.0%

: 108-24-7
acetic anhydride

: 80482-95-7
methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

: 80482-98-0
methyl 1,trans-2-diacetoxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

Guidance literature:: With dmap; In dichloromethane; for 96h;
DOI:10.1021/ja00368a015

Reference yield:

: 80482-95-7
methyl 1,trans-2-dihydroxy-cis-3-methyl-5-methylenecyclohexanecarboxylate

: 80483-01-8
methyl 1,trans-2-diacetoxy-cis-3-methyl-5-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 4-(N,N-dimethylamine)pyridine / CH₂Cl₂ / 96 h

2: 1.) O₃, 2.) zinc dust / 1.) -78 deg C, 2.) acetic acid, room temperature, 1 h

With dmap; ozone; zinc; In dichloromethane;
DOI:10.1021/ja00368a015