Technology Process of C14H8BrF4NO
There total 4 articles about C14H8BrF4NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
diethyl ether;
at -5 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diethylamino-sulfur trifluoride / dichloromethane / 0 - 20 °C / Inert atmosphere
2.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 °C / Inert atmosphere
3.1: diethyl ether / -5 - 20 °C
With
n-butyllithium; diethylamino-sulfur trifluoride;
In
diethyl ether; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / hexane; diethyl ether / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 0 °C / Inert atmosphere
2.1: diethylamino-sulfur trifluoride / dichloromethane / 0 - 20 °C / Inert atmosphere
3.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
3.2: 2 h / -78 °C / Inert atmosphere
4.1: diethyl ether / -5 - 20 °C
With
n-butyllithium; diethylamino-sulfur trifluoride;
In
diethyl ether; hexane; dichloromethane;