4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one

Base Information

Chemical Name:4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one
CAS No.:950503-06-7
Molecular Formula:C₂₆H₂₉N₃O₄S
Molecular Weight:479.6
Hs Code.:

Synonyms:4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one

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Chemical Property of 4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one

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Technology Process of 4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one

There total 10 articles about 4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356073-09-0
C₂₂H₂₇NO₄

: 950503-06-7
4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium cyanoborohydride / methanol / 20 °C

2: trifluoroacetic acid / 20 °C

With hydrogenchloride; sodium cyanoborohydride; trifluoroacetic acid; In methanol;
DOI:10.1016/j.bmcl.2011.10.049

Reference yield:

: 141337-05-5
2-(3-(bromomethyl)phenyl)ethanol

: 950503-06-7
4-hydroxy-7-[1R-hydroxy-2-(2-{3-[(2-methoxy-benzylamino)-methyl]-phenyl}-ethylamino)-ethyl]-3H-benzothiazol-2-one

Guidance literature:: Multi-step reaction with 7 steps

1: 2-nitropropane; sodium ethanolate / ethanol / 20 °C

2: toluene-4-sulfonic acid / toluene / Reflux

3: sodium tetrahydroborate / ethanol / 20 °C

4: dichloromethane

5: Dess-Martin periodane / dichloromethane / 20 °C

6: hydrogenchloride; sodium cyanoborohydride / methanol / 20 °C

7: trifluoroacetic acid / 20 °C

With hydrogenchloride; sodium tetrahydroborate; 2-nitropropane; sodium ethanolate; sodium cyanoborohydride; Dess-Martin periodane; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; ethanol; dichloromethane; toluene; 1: Hass-Bender reaction / 5: Dess-Martin oxidation;
DOI:10.1016/j.bmcl.2011.10.049