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Technology Process of 4-NO2C6H4SbO

4-NO2C6H4SbO

Base Information
  • Chemical Name:4-NO2C6H4SbO
  • CAS No.:874522-60-8
  • Molecular Formula:C6H4NO3Sb
  • Molecular Weight:259.853
  • Hs Code.:
4-NO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>SbO

Synonyms:4-NO2C6H4SbO

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Chemical Property of 4-NO2C6H4SbO
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Technology Process of 4-NO2C6H4SbO

There total 2 articles about 4-NO2C6H4SbO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-nitrophenyldichlorostibine
112995-72-9

4-nitrophenyldichlorostibine

4-NO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>SbO
874522-60-8

4-NO2C6H4SbO

Guidance literature:
With sodium hydroxide; hydrolysis with aq. NaOH at 0°C;
DOI:10.1021/ja01163a062

Reference yield: 58.0%

{4-NO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>}SbCl<sub>4</sub>
91159-51-2

{4-NO2C6H4N2}SbCl4

4-NO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>SbO
874522-60-8

4-NO2C6H4SbO

Guidance literature:
With zinc; In ethyl acetate; reduction at 65°C then hydrolysis;

Reference yield: 67.0%

4-NO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>SbO
874522-60-8

4-NO2C6H4SbO

{4-CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>}FeCl<sub>4</sub>

{4-CH3C6H4N2}FeCl4

{4-CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>N<sub>2</sub>}(4-NO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>SbCl<sub>3</sub>)

{4-CH3C6H4N2}(4-NO2C6H4SbCl3)

Guidance literature:
In ethanol; acetone; educt dissolving in ethanolic HCl, treating with diazonium salt in acetone;
upstream raw materials:

4-nitrophenyldichlorostibine

{4-NO2C6H4N2}SbCl4

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