C₃₈H₃₈O₁₁

Base Information

Chemical Name:C₃₈H₃₈O₁₁
CAS No.:1402931-89-8
Molecular Formula:C₃₈H₃₈O₁₁
Molecular Weight:670.713
Hs Code.:

C<sub>38</sub>H<sub>38</sub>O<sub>11</sub>

Synonyms:C₃₈H₃₈O₁₁

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Chemical Property of C₃₈H₃₈O₁₁

Chemical Property:

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Technology Process of C₃₈H₃₈O₁₁

There total 17 articles about C₃₈H₃₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960365-65-5
(1R,2R,3S,3aR,8bS)-methyl 1,6,8b-trihydroxy-8-methoxy-3a-(4-methoxyphenyl)-3-phenyl-2,3,3a,8b-tetrahydro-1H-benzo[b]-cyclopenta[d]furan-2-carboxylate

: 1402931-89-8
C₃₈H₃₈O₁₁

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / toluene / 0.17 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere; Molecular sieve

2.1: lithium hydroxide / methanol; water / 16 h / 45 °C / Inert atmosphere

2.2: pH 5 - 6 / Inert atmosphere

With triphenylphosphine; lithium hydroxide; In methanol; water; toluene;
DOI:10.1021/jm3011542

Reference yield:

: 1402931-82-1
C₃₉H₄₀O₁₁

: 1402931-89-8
C₃₈H₃₈O₁₁

Guidance literature:: C₃₉H₄₀O₁₁; With lithium hydroxide; In methanol; water; at 45 ℃; for 16h; Inert atmosphere;

With hydrogenchloride; In methanol; water; pH=5 - 6; Inert atmosphere;
DOI:10.1021/jm3011542

Reference yield:

: [2-[4-benzyloxy-2-methoxy-6-(4-methoxybenzoyl)oxyphenyl]-2-oxoethyl] 4-methoxybenzoate

: 1402931-89-8
C₃₈H₃₈O₁₁

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -70 - -20 °C / Inert atmosphere

2.1: sulfuric acid; acetic acid / 20 h / 20 °C / Inert atmosphere

3.1: water; sodium hydroxide / ethanol / 1 h / 80 °C / Inert atmosphere

4.1: methanol; dichloromethane; acetonitrile / 10 h / 0 - 5 °C / Inert atmosphere; UV-irradiation

4.2: 1 h / 60 °C / Inert atmosphere

4.3: 48 h / Inert atmosphere

5.1: 5%-palladium/activated carbon; hydrogen / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

6.1: ChiralPak AD-H / ethanol / Inert atmosphere; Supercritical conditions; Resolution of racemate

7.1: triphenylphosphine / toluene / 0.17 h / 0 °C / Inert atmosphere

7.2: 2 h / 0 °C / Inert atmosphere; Molecular sieve

8.1: lithium hydroxide / methanol; water / 16 h / 45 °C / Inert atmosphere

8.2: pH 5 - 6 / Inert atmosphere

With sulfuric acid; 5%-palladium/activated carbon; water; hydrogen; acetic acid; triphenylphosphine; sodium hydroxide; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; acetonitrile; 1.1: |Baker-Venkataraman Rearrangement;
DOI:10.1021/jm3011542