3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene
CAS No.:1314022-96-2
Molecular Formula:C₂₈H₁₆BBr₂F₅N₂O₄
Molecular Weight:710.057
Hs Code.:

Synonyms:3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

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Chemical Property of 3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

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Technology Process of 3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

There total 2 articles about 3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

: 1314022-96-2
3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

Guidance literature:: With bromine; iodine; In dichloromethane; at 40 ℃; for 12h;
DOI:10.1021/ol2014076

Reference yield:

: 956296-91-6
C₂₈H₁₉F₃N₂O₄

: 1314022-96-2
3,7-dibromo-2,8-di(4-methoxyphenyl)-11-trifluoromethyl-difuro[2,3-b]-[3,2-g]-5,5-difluoro-5-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate; triethylamine / 80 °C

2: bromine; iodine / dichloromethane / 12 h / 40 °C

With boron trifluoride diethyl etherate; bromine; iodine; triethylamine; In dichloromethane;
DOI:10.1021/ol2014076