C₂₃H₃₁NO₂S₂

Base Information

Chemical Name:C₂₃H₃₁NO₂S₂
CAS No.:1372122-72-9
Molecular Formula:C₂₃H₃₁NO₂S₂
Molecular Weight:417.637
Hs Code.:

C<sub>23</sub>H<sub>31</sub>NO<sub>2</sub>S<sub>2</sub>

Synonyms:C₂₃H₃₁NO₂S₂

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Chemical Property of C₂₃H₃₁NO₂S₂

Chemical Property:

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Technology Process of C₂₃H₃₁NO₂S₂

There total 1 articles about C₂₃H₃₁NO₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1118-59-8
3-methylbut-3-en-1-al

: 1372122-72-9
C₂₃H₃₁NO₂S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 12 h / -78 °C / Inert atmosphere

2.1: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - -20 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ol3007259

Reference yield: 85.0%

: 1372122-72-9
C₂₃H₃₁NO₂S₂

: 1372122-74-1
C₁₇H₂₄O₂

Guidance literature:: With methanol; lithium borohydride; In diethyl ether; at 0 - 20 ℃;
DOI:10.1021/ol3007259

Reference yield:

: 1372122-72-9
C₂₃H₃₁NO₂S₂

: 1372122-81-0
C₂₁H₂₈O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: methanol; lithium borohydride / diethyl ether / 0 - 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C / Inert atmosphere

3.1: osmium(VIII) oxide; N,N,N,N,-tetramethylethylenediamine / dichloromethane / 14 h / -78 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere

5.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve

6.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere

6.2: -78 °C / Inert atmosphere

7.1: mercury(II) perchlorate tetrahydrate; water; calcium carbonate / tetrahydrofuran / 0.01 h / 0 °C

8.1: perchloric acid / dichloromethane / 0.17 h / 0 °C

9.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / Inert atmosphere; Molecular sieve

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; osmium(VIII) oxide; lithium borohydride; n-butyllithium; perchloric acid; tetrapropylammonium perruthenate; mercury(II) perchlorate tetrahydrate; N,N,N,N,-tetramethylethylenediamine; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; calcium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1021/ol3007259