C₄₇H₇₇NO₂

Base Information

• Chemical Name: C₄₇H₇₇NO₂
• CAS No.: 1010685-24-1
• Molecular Formula: C₄₇H₇₇NO₂
• Molecular Weight: 688.134
• Mol file: 1010685-24-1.mol

Synonyms:C₄₇H₇₇NO₂

Chemical Property of C₄₇H₇₇NO₂

Chemical Property:

Purity/Quality:

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Technology Process of C₄₇H₇₇NO₂

There total 1 articles about C₄₇H₇₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

1-dodecyne (765-03-7) + C35H56BrNO2 (1010685-23-0) → C47H77NO2 (1010685-24-1)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 100 ℃; for 36h; Inert atmosphere;

DOI:10.1039/b714291a

Reference yield: 95.0%

C47H77NO2 (1010685-24-1) → C47H81NO2 (1010685-25-2)

Guidance literature:

With Pd/C; hydrogen; In ethyl acetate; for 12h; under 2327.23 Torr; Autoclave;

DOI:10.1039/b714291a

upstream raw materials:

1-dodecyne

C₃₅H₅₆BrNO₂

Downstream raw materials:

C₄₇H₈₁NO₂