1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

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Chemical Name:1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose
CAS No.:102871-19-2
Molecular Formula:C₃₄H₄₀O₁₄
Molecular Weight:672.683
Hs Code.:

Synonyms:1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

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Chemical Property of 1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

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Technology Process of 1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

There total 1 articles about 1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 67965-18-8
3,4-di-O-Benzyl-1,6-anhydro-β-L-gulopyranose

: 572-10-1,4451-35-8,4451-36-9,14227-52-2,14227-87-3,14227-88-4,14257-40-0,17081-03-7,19186-60-8,57237-01-1,65982-17-4,65982-18-5,65982-19-6,66966-08-3,144299-57-0
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl chloride

: 102871-19-2
1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; at 25 ℃; for 14h;
DOI:10.1021/jo00365a013

Reference yield:

: 108-24-7
acetic anhydride

: 102871-19-2
1,6-anhydro-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

: 102919-87-9
1,6-di-O-acetyl-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-L-gulopyranose

: 102871-15-8
1,6-di-O-acetyl-3,4-di-O-benzyl-2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-β-L-gulopyranose

Guidance literature:: With sulfuric acid; acetic acid; at 0 ℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00365a013