C₃₂H₃₆N₆O₅S

Base Information

Chemical Name:C₃₂H₃₆N₆O₅S
CAS No.:1346673-01-5
Molecular Formula:C₃₂H₃₆N₆O₅S
Molecular Weight:616.741
Hs Code.:

C<sub>32</sub>H<sub>36</sub>N<sub>6</sub>O<sub>5</sub>S

Synonyms:C₃₂H₃₆N₆O₅S

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Chemical Property of C₃₂H₃₆N₆O₅S

Chemical Property:

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Technology Process of C₃₂H₃₆N₆O₅S

There total 16 articles about C₃₂H₃₆N₆O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1346673-00-4
6-chloro-4-(5-(2-hydroxypropan-2-yl)-1-methyl-1H-pyrazol-3-ylamino)-2-methylpyridazin-3(2H)-one

: 1346672-79-4
2-(1-oxo-3,4,5,6,7,8-hexahydrobenzothieno[2,3-c]pyridin-2(1H)-yl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl acetate

: 1346673-01-5
C₃₂H₃₆N₆O₅S

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 130 ℃; for 0.416667h; Inert atmosphere; microwave irradiation;

Reference yield:

: 40133-07-1
4,5,6,7-tetrahydrobenzo[b]thiophene-2-carboxylic acid

: 1346673-01-5
C₃₂H₃₆N₆O₅S

Guidance literature:: Multi-step reaction with 10 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3: tetrahydrofuran / 4 h / -10 - 0 °C / Inert atmosphere

4: hydrogenchloride / dichloromethane; diethyl ether / 1 h / 20 °C

5: sulfuric acid / 16 h / 95 °C

6: hydroxylamine hydrochloride; sodium acetate / methanol / 16 h / 20 °C / Inert atmosphere

7: polyphosphoric acid / 16 h / 80 °C / Inert atmosphere

8: caesium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

9: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 90 °C / Inert atmosphere

10: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.42 h / 130 °C / Inert atmosphere; microwave irradiation

With hydrogenchloride; oxalyl dichloride; sulfuric acid; hydroxylamine hydrochloride; potassium acetate; sodium acetate; sodium carbonate; caesium carbonate; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane;

Reference yield:

: 65361-26-4
4,5,6,7-tetrahydrobenzo[b]thiophene-2-carboxylic acid chloride

: 1346673-01-5
C₃₂H₃₆N₆O₅S

Guidance literature:: Multi-step reaction with 9 steps

1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

2: tetrahydrofuran / 4 h / -10 - 0 °C / Inert atmosphere

3: hydrogenchloride / dichloromethane; diethyl ether / 1 h / 20 °C

4: sulfuric acid / 16 h / 95 °C

5: hydroxylamine hydrochloride; sodium acetate / methanol / 16 h / 20 °C / Inert atmosphere

6: polyphosphoric acid / 16 h / 80 °C / Inert atmosphere

7: caesium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

8: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 90 °C / Inert atmosphere

9: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 0.42 h / 130 °C / Inert atmosphere; microwave irradiation

With hydrogenchloride; sulfuric acid; hydroxylamine hydrochloride; potassium acetate; sodium acetate; sodium carbonate; caesium carbonate; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane;