N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

Base Information

Chemical Name:N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine
CAS No.:107961-42-2
Molecular Formula:C₂₆H₃₂N₆O₇
Molecular Weight:540.576
Hs Code.:

N<sup>6</sup>-benzoyl-5'(S)-C-<<N-(tert-butyloxycarbonyl)amino>methyl>-2',3'-O-isopropylideneadenosine

Synonyms:N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

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Chemical Property of N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

Chemical Property:

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Technology Process of N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

There total 7 articles about N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 107961-45-5
N⁶-benzoyl-5'(R)-C-<methyl>-2',3'-O-isopropylidene-5'-O-(p-toluenesulfonyl)adenosine

: 107961-42-2
N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

Guidance literature:: With potassium nitrite; In dimethyl sulfoxide; at 85 - 90 ℃; for 12h;
DOI:10.1021/jm00388a024

Reference yield:

: 84757-76-6
N⁶-benzoyl-5'(S)-C-(nitromethyl)-2',3'-O-isopropylideneadenosine

: 107961-42-2
N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / methanol / 16 h / 20 °C / 2585.7 Torr

2: CH₂Cl₂ / 1 h / 20 °C

With hydrogen; platinum(IV) oxide; In methanol; dichloromethane;
DOI:10.1021/jm00388a024

Reference yield:

: 84757-69-7
N⁶-benzoyl-5'(R)-C-(nitromethyl)-2',3'-O-isopropylideneadenosine

: 107961-42-2
N⁶-benzoyl-5'(S)-C-<methyl>-2',3'-O-isopropylideneadenosine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / PtO₂ / methanol / 16 h / 20 °C / 2585.7 Torr

2: CH₂Cl₂ / 1 h / 20 °C

3: 85 percent / pyridine / 28 h / 20 °C

4: 48 percent / KNO₂ / dimethylsulfoxide / 12 h / 85 - 90 °C

With pyridine; potassium nitrite; hydrogen; platinum(IV) oxide; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00388a024