3-iodopropyl thiocyanate

Base Information

• Chemical Name: 3-iodopropyl thiocyanate
• CAS No.: 1453200-86-6
• Molecular Formula: C₄H₆INS
• Molecular Weight: 227.069
• Mol file: 1453200-86-6.mol

Synonyms:3-iodopropyl thiocyanate

Chemical Property of 3-iodopropyl thiocyanate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-iodopropyl thiocyanate

There total 1 articles about 3-iodopropyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

3-chloropropyl thiocyanate (53310-50-2) → 1,3-Diiodopropane (627-31-6) + 1,3-bis(thiocyanato)propane (7314-74-1) + 3-iodopropyl thiocyanate (1453200-86-6)

Guidance literature:

With sodium iodide; In acetone; for 24h; Reflux;

DOI:10.3762/bjoc.9.115

Reference yield: 28.0%

3-iodopropyl thiocyanate (1453200-86-6) + silver(I) 4-methylbenzenesulfonate (16836-95-6) → 3-(toluenesulfonyloxy)propyl thiocyanate (1107610-26-3)

Guidance literature:

In acetonitrile; at 20 ℃; for 27h; Darkness;

DOI:10.3762/bjoc.9.115

Reference yield: 22.0%

3-iodopropyl thiocyanate (1453200-86-6) + Silver 4-nitrobenzene sulfonate (39938-18-6) → C10H10N2O5S2 (1453200-85-5)

Guidance literature:

In acetonitrile; at 20 ℃; for 27h; Darkness;

DOI:10.3762/bjoc.9.115

upstream raw materials:

3-chloropropyl thiocyanate

Downstream raw materials:

3-(toluenesulfonyloxy)propyl thiocyanate

C₁₀H₁₀N₂O₅S₂

Refernces