C₁₃H₁₅ClO₄

Base Information

• Chemical Name: C₁₃H₁₅ClO₄
• CAS No.: 1364301-63-2
• Molecular Formula: C₁₃H₁₅ClO₄
• Molecular Weight: 270.713
• Mol file: 1364301-63-2.mol

Synonyms:C₁₃H₁₅ClO₄

Chemical Property of C₁₃H₁₅ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₅ClO₄

There total 1 articles about C₁₃H₁₅ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-iodo-2-chloropropene (39557-31-8) + 2-iodo-4,5-dimethoxybenzoic acid methyl ester (173043-61-3) → C13H15ClO4 (1364301-63-2)

Guidance literature:

2-iodo-4,5-dimethoxybenzoic acid methyl ester; With isopropylmagnesium bromide; In tetrahydrofuran; at -40 ℃; for 0.5h; Inert atmosphere;

With copper(l) cyanide; lithium chloride; In tetrahydrofuran; at -40 ℃; for 0.0833333h; Inert atmosphere;

3-iodo-2-chloropropene; In tetrahydrofuran; at -40 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.01.011

Reference yield:

C13H15ClO4 (1364301-63-2) → C12H13ClO4 (1364301-73-4)

Guidance literature:

C₁₃H₁₅ClO₄; With sodium hydroxide; In methanol; water; at 20 ℃; for 20h;

With hydrogenchloride; In water; pH=2;

DOI:10.1016/j.tetlet.2012.01.011

upstream raw materials:

3-iodo-2-chloropropene

2-iodo-4,5-dimethoxybenzoic acid methyl ester

Downstream raw materials:

C₁₂H₁₃ClO₄