2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 81098-51-3
• Molecular Formula: C₂₅H₂₃ClN₃O₄P₃
• Molecular Weight: 557.85

Synonyms:2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property:

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Technology Process of 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 4 articles about 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

6-Methyl-2,2,4,4-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-42-2) → 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-51-3)

Guidance literature:

With chlorine; In tetrachloromethane; at 0 ℃; for 0.0833333h;

DOI:10.1021/ja00373a024

Reference yield:

sodium phenoxide (139-02-6) → 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / tetrahydrofuran / 24 h / Heating

2: 45 percent / Cl₂ / CCl₄ / 0.08 h / 0 °C

With chlorine; In tetrahydrofuran; tetrachloromethane;

DOI:10.1021/ja00373a024

Reference yield:

1,1'-dimethyl-3,3,3',3',5,5,5',5'-octaphenoxybi(cyclotriphosphazene) (81098-44-4) → 2-Chloro-2-methyl-4,4,6,6-tetraphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (81098-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 27 percent / tetrahydrofuran / 48 h / Heating

2: 45 percent / Cl₂ / CCl₄ / 0.08 h / 0 °C

With chlorine; In tetrahydrofuran; tetrachloromethane;

DOI:10.1021/ja00373a024

upstream raw materials:

sodium 2,2,2-trifluoroethanolate

1,1'-dimethyl-3,3,3',3',5,5,5',5'-octaphenoxybi(cyclotriphosphazene)

6-Methyl-2,2,4,4-tetraphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

sodium phenoxide

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