(6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

Base Information

• Chemical Name: (6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester
• CAS No.: 33741-92-3
• Molecular Formula: C₃₄H₃₅N₃O₇S
• Molecular Weight: 629.734

Synonyms:(6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

Chemical Property of (6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

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Technology Process of (6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

There total 2 articles about (6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester (33741-92-3)

Guidance literature:

3-Acetoxymethyl-7ss-ceph-3-em-4-carbonsaeure,Enzy-mat. Desacetylieren, Diphenyldiazomethan;

Reference yield:

→ (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester (33741-92-3)

Guidance literature:

Entspr. Carbonsaeure, Diphenyldiazomethan;

Reference yield: 94.0%

(6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-hydroxymethyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester (33741-92-3) → (6R,7R)-7-(2-tert-Butoxycarbonylamino-2-phenyl-acetylamino)-3-formyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

Guidance literature:

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; for 12h; Ambient temperature;

DOI:10.1021/jo00127a036

Downstream raw materials:

[(R)-((5aR)-1,7-dioxo-(5ar)-1,4,6,7-tetrahydro-3H,5aH-azeto[2,1-b]furo[3,4-d][1,3]thiazin-6t-ylcarbamoyl)-phenyl-methyl]-carbamic acid tert-butyl ester

(6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-formyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-3-ene-2c-carboxylic acid benzhydryl ester

(6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-formyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

(6R)-7t-((R)-2-amino-2-phenyl-acetylamino)-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

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