10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

Base Information

Chemical Name:10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide
CAS No.:1014987-21-3
Molecular Formula:C₁₃H₁₈N₂O₅S₂
Molecular Weight:346.428
Hs Code.:

Synonyms:10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

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Chemical Property of 10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

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Technology Process of 10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

There total 4 articles about 10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 914082-71-6
2-sulfamoyloxymethyl-1-(toluene-4-sulfonyl)-piperidine

: 1014987-21-3
10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

Guidance literature:: With [bis(acetoxy)iodo]benzene; magnesium oxide; dirhodium tetraacetate; In dichloromethane; at 40 ℃;
DOI:10.1021/ol061649x

Reference yield:

: 60343-64-8
[1-(toluene-4-sulfonyl)piperidin-2-yl]methanol

: 1014987-21-3
10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 496 mg / ClSO₂NH₂; pyridine / CH₂Cl₂ / 0 - 20 °C

2: 67 percent / PhI(OAc)2; MgO / Rh₂(OAc)4 / CH₂Cl₂ / 40 °C

With pyridine; [bis(acetoxy)iodo]benzene; sulphamoyl chloride; magnesium oxide; dirhodium tetraacetate; In dichloromethane; 2: Du Bois reaction;
DOI:10.1021/ol061649x

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1014987-21-3
10-(toluene-4-sulfonyl)-4-oxa-3-thia-2,10-diaza-bicyclo[4.3.1]decane 3,3-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: acetone; H₂O / 20 °C

2: 496 mg / ClSO₂NH₂; pyridine / CH₂Cl₂ / 0 - 20 °C

3: 67 percent / PhI(OAc)2; MgO / Rh₂(OAc)4 / CH₂Cl₂ / 40 °C

With pyridine; [bis(acetoxy)iodo]benzene; sulphamoyl chloride; magnesium oxide; dirhodium tetraacetate; In dichloromethane; water; acetone; 3: Du Bois reaction;
DOI:10.1021/ol061649x