4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

Base Information

Chemical Name:4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide
CAS No.:137208-00-5
Molecular Formula:C₂₀H₁₉ClN₂O₄
Molecular Weight:386.835
Hs Code.:

4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N<sup>2</sup>-oxide

Synonyms:4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

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Chemical Property of 4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

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Technology Process of 4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

There total 5 articles about 4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.4%

: 124397-52-0
4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine

: 137208-00-5
4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 80 ℃; for 2h;
DOI:10.1248/cpb.39.2009

Reference yield:

: 578-57-4
2-bromoanisole

: 137208-00-5
4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 1a) Mg, 1b) CdCl₂ / 1a) ether, 1b) 30 min, r.t., 2) THF, 1 h, reflux

2: hydrazine hydrate / ethanol / 2 h / 80 °C

3: 85.7 percent / POCl₃ / 0.5 h / Heating

4: 54.4 percent / H₂O₂ / acetic acid / 2 h / 80 °C

With dihydrogen peroxide; hydrazine hydrate; magnesium; cadmium(II) chloride; trichlorophosphate; In ethanol; acetic acid;
DOI:10.1248/cpb.39.2009

Reference yield:

: 56611-62-2
3,5-dimethyl-4-ethoxycarbonyl-phthalic anhydride

: 137208-00-5
4-(2-anisyl)-1-chloro-7-ethoxycarbonyl-6,8-dimethylphthalazine N²-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 1a) Mg, 1b) CdCl₂ / 1a) ether, 1b) 30 min, r.t., 2) THF, 1 h, reflux

2: hydrazine hydrate / ethanol / 2 h / 80 °C

3: 85.7 percent / POCl₃ / 0.5 h / Heating

4: 54.4 percent / H₂O₂ / acetic acid / 2 h / 80 °C

With dihydrogen peroxide; hydrazine hydrate; magnesium; cadmium(II) chloride; trichlorophosphate; In ethanol; acetic acid;
DOI:10.1248/cpb.39.2009