3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:1402905-80-9
Molecular Formula:C₃₁H₃₃ClN₂O₁₅S
Molecular Weight:741.126
Hs Code.:

Synonyms:3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Chemical Property of 3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Technology Process of 3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 3 articles about 3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 16977-81-4
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-bromopropoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1402905-79-6
3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenol

: 1402905-80-9
3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: 3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenol; With potassium carbonate; In N,N-dimethyl-formamide; for 0.5h;

(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(3-bromopropoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/cmdc.201200224

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 1402905-80-9
3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Molecular sieve

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

2.2: 20 °C

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200224

Reference yield:

: 601-89-8
2-nitroresorcinol

: 1402905-80-9
3-(3-{[5-(5-chlorothiophen-2-yl)isoxazol-3-yl]methoxy}-2-nitrophenoxy)propyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h

2.2: 20 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200224