(+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

Base Information

Chemical Name:(+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol
CAS No.:142096-79-5
Molecular Formula:C₁₂H₁₆O
Molecular Weight:176.258
Hs Code.:

Synonyms:(+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

Chemical Property:

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Technology Process of (+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

There total 21 articles about (+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-11-6
diiodomethane

: 75553-23-0
(E)-5-phenyl-2-penten-1-ol

: 142096-79-5
(-)-(1R,2R)-2-(2-phenylethyl)cyclopropylmethanol

: 142096-79-5
(+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

Guidance literature:: With diethylzinc; (S)-MsNHCH(PhCH₂)CH₂NHSO₂C₆H₄-p-NO₂; In hexane; dichloromethane; at -23 ℃; for 20h; Product distribution; various allylic alcohols and chiral disulfonamides;
DOI:10.1016/S0040-4039(97)00038-5

Reference yield:

: 75-11-6
diiodomethane

: 75553-23-0
(E)-5-phenyl-2-penten-1-ol

: 142096-79-5
(-)-(1R,2R)-2-(2-phenylethyl)cyclopropylmethanol

: 142096-79-5
(+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

Guidance literature:: With diethylzinc; (S)-MsNHCH(PhCH₂)CH₂NHSO₂C₆H₄-p-NO₂; In hexane; dichloromethane; at -23 ℃; for 20h; Product distribution; various allylic alcohols and chiral disulfonamides;
DOI:10.1016/S0040-4039(97)00038-5

Reference yield:

: 75553-23-0
(E)-5-phenyl-2-penten-1-ol

: 14399-53-2
bis(iodomethyl)zinc

: 142096-79-5
(-)-(1R,2R)-2-(2-phenylethyl)cyclopropylmethanol

: 142096-79-5
(+)-(1S,2S)-2-(2-phenylethyl)cyclopropylmethanol

Guidance literature:: With dioxabutylborolane of (R,R)-N,N,N',N'-tetramethyltartaric acid diamide; In dichloromethane; for 8h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/ja982055v