N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

Base Information

Chemical Name:N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide
CAS No.:1335015-25-2
Molecular Formula:C₂₃H₁₄BrN₃O₃
Molecular Weight:460.286
Hs Code.:

Synonyms:N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

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Chemical Property of N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

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Technology Process of N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

There total 5 articles about N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: C₁₆H₆BrClN₂O₃

: 100-46-9
benzylamine

: 1335015-25-2
N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

Guidance literature:: With dmap; In chloroform; for 5h; Reflux;
DOI:10.1016/j.ejmech.2011.07.042

Reference yield:

: 626-55-1,163928-56-1
3-Bromopyridine

: 1335015-25-2
N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 5 h / Reflux

2.1: potassium carbonate / water; isopropyl alcohol / 24 h / Reflux

2.2: pH 3

3.1: thionyl chloride; triethylamine / chloroform / 5 h / Reflux

4.1: dmap / chloroform / 5 h / Reflux

With dmap; thionyl chloride; potassium carbonate; triethylamine; In ethanol; chloroform; water; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.07.042

Reference yield:

: 1310457-53-4
ethyl 9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxylate

: 1335015-25-2
N-benzyl-9-bromo-5,12-dioxo-5,12-dihydroindolizino[2,3-g]quinoline-6-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / water; isopropyl alcohol / 24 h / Reflux

1.2: pH 3

2.1: thionyl chloride; triethylamine / chloroform / 5 h / Reflux

3.1: dmap / chloroform / 5 h / Reflux

With dmap; thionyl chloride; potassium carbonate; triethylamine; In chloroform; water; isopropyl alcohol;
DOI:10.1016/j.ejmech.2011.07.042