N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Base Information

Chemical Name:N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide
CAS No.:1584679-92-4
Molecular Formula:C₂₃H₂₉N₅O₃S
Molecular Weight:455.581
Hs Code.:

Synonyms:N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

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Technology Process of N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

There total 3 articles about N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1584679-81-1
N-[5-(cyanomethyl)-1,3,4-thiadiazol-2-yl]dodecanamide

: 555-16-8
4-nitrobenzaldehdye

: 1584679-92-4
N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Guidance literature:: With piperidine; In ethanol; for 0.166667h; Reflux;
DOI:10.1080/00397911.2013.846381

Reference yield:

: 1584679-80-0
1-(2-cyanoacetyl)-4-dodecanoyl thiosemicarbazide

: 1584679-92-4
N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 1.17 h / 0 °C

2: piperidine / ethanol / 0.17 h / Reflux

With piperidine; sulfuric acid; In ethanol;
DOI:10.1080/00397911.2013.846381

Reference yield:

: 112-16-3
n-dodecanoyl chloride

: 1584679-92-4
N-(5-(1-cyano-2-(4-nitrophenyl)vinyl)-1,3,4-thiadiazol-2-yl)dodecanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-dioxane / 0.5 h / Reflux

2: 2 h / Reflux

3: piperidine / ethanol / 0.17 h / Reflux

With piperidine; In 1,4-dioxane; ethanol;
DOI:10.1080/00397911.2013.846381