C₁₅H₂₄O₄SSi

Base Information

Chemical Name:C₁₅H₂₄O₄SSi
CAS No.:1338989-40-4
Molecular Formula:C₁₅H₂₄O₄SSi
Molecular Weight:328.505
Hs Code.:

C<sub>15</sub>H<sub>24</sub>O<sub>4</sub>SSi

Synonyms:C₁₅H₂₄O₄SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₄O₄SSi

Chemical Property:

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Technology Process of C₁₅H₂₄O₄SSi

There total 10 articles about C₁₅H₂₄O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1338989-91-5
C₁₅H₂₆O₄SSi

: 1338989-40-4
C₁₅H₂₄O₄SSi

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 25 ℃;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: C₁₂H₁₂O₂S

: 1338989-40-4
C₁₅H₂₄O₄SSi

Guidance literature:: Multi-step reaction with 9 steps

1: sodium thiophenolate / methanol / 23 °C

2: copper(l) iodide / tetrahydrofuran / -78 °C

3: diisobutylaluminium hydride / dichloromethane / 0 °C

4: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / -15 °C

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C

6: lithium aluminium tetrahydride / tetrahydrofuran / 25 °C

7: 2,6-dimethylpyridine / dichloromethane / -40 °C

8: methanol; potassium carbonate / -15 °C

9: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 25 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; copper(l) iodide; lithium aluminium tetrahydride; hexaammonium heptamolybdate tetrahydrate; diethyl (2R,3R)-tartrate; dihydrogen peroxide; sodium thiophenolate; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; ethanol; dichloromethane; 5: Katsuki-Sharpless asymmetric epoxidation / 9: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: 73311-79-2
C₁₃H₁₆O₂S

: 1338989-40-4
C₁₅H₂₄O₄SSi

Guidance literature:: Multi-step reaction with 7 steps

1: diisobutylaluminium hydride / dichloromethane / 0 °C

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / -15 °C

3: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 25 °C

5: 2,6-dimethylpyridine / dichloromethane / -40 °C

6: methanol; potassium carbonate / -15 °C

7: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 25 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; lithium aluminium tetrahydride; hexaammonium heptamolybdate tetrahydrate; diethyl (2R,3R)-tartrate; dihydrogen peroxide; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; ethanol; dichloromethane; 3: Katsuki-Sharpless asymmetric epoxidation / 7: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2011.08.051