ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

Base Information

Chemical Name:ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate
CAS No.:935760-48-8
Molecular Formula:C₁₅H₁₁ClN₂O₃S
Molecular Weight:334.783
Hs Code.:

Synonyms:ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

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Chemical Property of ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

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Technology Process of ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

There total 2 articles about ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 65234-09-5
ethyl 2-amino-4-chlorophenyl-thiophene-3-carboxylate

: 623-49-4
ethyl cyanoformate

: 935760-48-8
ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

Guidance literature:: With hydrogenchloride; In acetic acid; at 90 ℃; for 10h;
DOI:10.1021/acs.jmedchem.6b01007

Reference yield: 86.0%

: 935760-48-8
ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

Guidance literature:

Reference yield:

: 935760-48-8
ethyl 5-(4-chlorophenyl)-4-oxo-3,4-dihydrothieno[2,3-d]-pyrimidine-2-carboxylate

: 935760-22-8
1-{3-[(2-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]oxy}-ethyl)oxy]phenyl}methanamine

: 935759-61-8
5-(4-chlorophenyl)-4-oxo-N-{3-[2-(1H-1,2,4-triazol-3-yloxy)-ethoxy]benzyl}-3,4-dihydro-thieno[2,3-d]pyrimidine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 96 h / 90 °C

2: triethylsilane; trifluoroacetic acid / acetonitrile / 3 h / 50 °C

With triethylsilane; trifluoroacetic acid; In ethanol; acetonitrile;
DOI:10.1021/acs.jmedchem.6b01007