methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside
CAS No.:866322-06-7
Molecular Formula:C₃₈H₄₄NO₁₀P
Molecular Weight:705.742
Hs Code.:

Synonyms:methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Suppliers and Price of methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

There total 2 articles about methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 88981-21-9
2-(N-benzyloxycarbonylamino)ethylphosphonic acid benzyl ester

: 17791-36-5
methyl 2,3-di-O-benzyl-α-D-glucopyranoside

: 866322-06-7
methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 40 ℃; for 3h;
DOI:10.1021/jo0508595

Reference yield:

: 88981-21-9
2-(N-benzyloxycarbonylamino)ethylphosphonic acid benzyl ester

: 866322-06-7
methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: DMF; oxalyl chloride / CH₂Cl₂ / 0.5 h / 0 °C

2: 75 percent / Et₃N / CH₂Cl₂ / 1 h / -10 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jo0508595

Reference yield: 85.0%

: 866322-06-7
methyl 6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

: 74666-83-4,105990-37-2,108739-67-9,125354-47-4,125411-99-6,125354-46-3
S-ethyl 2,3,4,6-tetra-O-benzyl-1-deoxy-1-thio-α-D-mannopyranoside

: 866322-09-0
methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)(1->4)-6-O-((2-benzyloxycarbonylaminoethyl)phosphonic acid benzyl ester)-2,3-di-O-benzyl-α-D-glucopyranoside

Guidance literature:: With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In diethyl ether; at 0 - 20 ℃; for 6h;
DOI:10.1021/jo0508595