3,5-dimethyl-2,4,6-trichlorobenzyl alkohol

Base Information

• Chemical Name: 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol
• CAS No.: 114634-33-2
• Molecular Formula: C₉H₉Cl₃O
• Molecular Weight: 239.529
• Mol file: 114634-33-2.mol

Synonyms:3,5-dimethyl-2,4,6-trichlorobenzyl alkohol

Chemical Property of 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol

There total 3 articles about 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,4,6-Trichloro-3,5-dimethyl-phenyl)-acetic acid methyl ester → 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol (114634-33-2)

Guidance literature:

With potassium hydroxide; In ethanol; for 4h; Yield given; Heating;

DOI:10.1021/jo00247a045

Reference yield:

1,3,5-trichloro-2,4,6-trimethylbenzene (5324-68-5) → 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol (114634-33-2)

Guidance literature:

Multi-step reaction with 3 steps

1: NBS / CCl₄ / 3 h / Irradiation

2: trioctylmethylammonium chloride / acetonitrile / 12 h / 70 °C

3: KOH / aq. ethanol / 4 h / Heating

With potassium hydroxide; N-Bromosuccinimide; Aliquat 336; In tetrachloromethane; ethanol; acetonitrile;

DOI:10.1021/jo00247a045

Reference yield:

1-Bromomethyl-2,4,6-trichloro-3,5-dimethyl-benzene → 3,5-dimethyl-2,4,6-trichlorobenzyl alkohol (114634-33-2)

Guidance literature:

Multi-step reaction with 2 steps

1: trioctylmethylammonium chloride / acetonitrile / 12 h / 70 °C

2: KOH / aq. ethanol / 4 h / Heating

With potassium hydroxide; Aliquat 336; In ethanol; acetonitrile;

DOI:10.1021/jo00247a045

upstream raw materials:

1,3,5-trichloro-2,4,6-trimethylbenzene

Downstream raw materials:

meso-tetrakis(3,5-dimethyl-2,4,6-trichlorophenyl)porphyrin

3,5-dimethyl-2,4,6-trichlorobenzaldehyde