6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

Base Information

Chemical Name:6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine
CAS No.:120524-34-7
Molecular Formula:C₂₂H₂₁ClN₄O₉S
Molecular Weight:552.949
Hs Code.:

Synonyms:6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

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Technology Process of 6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

There total 1 articles about 6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 92123-05-2
6-chloro-2-phenylthio-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

: 120524-34-7
6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

Guidance literature:: With potassium permanganate; In water; acetic acid; at 0 ℃; for 3h;
DOI:10.1021/jm00128a002

Reference yield: 81.0%

: 1003-03-8
Cyclopentamine

: 120524-34-7
6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

: 120524-35-8
N⁶-cyclopentyl-2-(phenylsulfonyl)adenosine 2',3',5'-triacetate

Guidance literature:: With triethylamine; In 1,2-dimethoxyethane; for 3h; Ambient temperature;
DOI:10.1021/jm00128a002

Reference yield:

: 120524-34-7
6-chloro-2-(phenylsulfonyl)-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

: 120524-37-0
N⁶-cyclohexyl-2-(phenylsulfonyl)adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / 1,2-dimethoxy-ethane / Ambient temperature

2: NH₃ / methanol / Ambient temperature

With ammonia; triethylamine; In methanol; 1,2-dimethoxyethane;
DOI:10.1021/jm00128a002