ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate

Base Information

Chemical Name:ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate
CAS No.:1207089-90-4
Molecular Formula:C₂₀H₂₀F₃N₅O₂
Molecular Weight:419.406
Hs Code.:

Synonyms:ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate

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Chemical Property of ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate

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Technology Process of ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate

There total 2 articles about ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 763129-56-2
1-(4-amino-3-methylbenzyl)-4-[4-(trifluoromethyl)phenyl]-1,4-dihydro-5H-tetrazol-5-one

: 78-39-7
Triethyl orthoacetate

: 1207089-90-4
ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate

Guidance literature:: toluene-4-sulfonic acid; at 60 ℃; for 0.5h;

Reference yield:

: 763129-59-5
1-(3-methyl-4-nitrobenzyl)-4-(4-trifluoromethyl-phenyl)-1,4-dihydrotetrazol-5-one

: 1207089-90-4
ethyl N-[2-methyl-4-({5-oxo-4-[4(trifluoromethyl)phenyl]-4,5-dihydro-1H-tetrazole-1-yl}methyl)phenyl]ethanimidate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C

2: toluene-4-sulfonic acid / 0.5 h / 60 °C

With hydrogen; palladium 10% on activated carbon; toluene-4-sulfonic acid; In ethanol;