C₃₆H₄₆N₅O₁₃PS

Base Information

Chemical Name:C₃₆H₄₆N₅O₁₃PS
CAS No.:1608113-65-0
Molecular Formula:C₃₆H₄₆N₅O₁₃PS
Molecular Weight:819.827
Hs Code.:

C<sub>36</sub>H<sub>46</sub>N<sub>5</sub>O<sub>13</sub>PS

Synonyms:C₃₆H₄₆N₅O₁₃PS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₄₆N₅O₁₃PS

Chemical Property:

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Technology Process of C₃₆H₄₆N₅O₁₃PS

There total 13 articles about C₃₆H₄₆N₅O₁₃PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1608113-17-2
N-For-Met-L-Glu-OMe

: 1608113-64-9
C₂₄H₂₈N₃O₈P

: 1608113-65-0
C₃₆H₄₆N₅O₁₃PS

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201301781

Reference yield:

: 287731-68-4
N-formyl-methionine-succinimidyl ester

: 1608113-65-0
C₃₆H₄₆N₅O₁₃PS

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 0 - 20 °C / 760.05 Torr

3: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere

With dmap; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301781

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 1608113-65-0
C₃₆H₄₆N₅O₁₃PS

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; dmap / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

2.1: triethylamine; methanesulfonyl chloride / 2 h / 20 °C / Inert atmosphere

2.2: 1.5 h / Inert atmosphere; Reflux

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 2 h / 0 - 20 °C / Inert atmosphere

4.1: acetic acid / 3 h / 20 °C / Inert atmosphere

5.1: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

5.2: 2 h / -40 - 20 °C / Inert atmosphere

6.1: methylamine / water; ethanol / 0.5 h / 0 - 20 °C

7.1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere

With 1H-tetrazole; dmap; di-isopropyl azodicarboxylate; acetic acid; methanesulfonyl chloride; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; methylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: |Mitsunobu Displacement;
DOI:10.1002/ejoc.201301781