phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

Base Information

Chemical Name:phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate
CAS No.:144876-63-1
Molecular Formula:C₂₈H₃₀N₄O₃
Molecular Weight:470.571
Hs Code.:

phenylmethyl <R-(R*,R*)>-<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

Synonyms:phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

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Chemical Property of phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

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Technology Process of phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

There total 3 articles about phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 144876-58-4
9H-fluoren-9-ylmethyl -3-(1H-indol-3-ylmethyl)-3-methyl-4,9-dioxo-7,11-diphenyl-10-oxa-2,5,8-triazaundecanoate

: 144876-63-1
phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 0 ℃; for 17h;
DOI:10.1016/S0040-4020(01)86596-0

Reference yield:

: 130406-36-9,142854-51-1
((S)-2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester

: 144876-63-1
phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / 1) THF, EtOAc, 25 deg C, 2 h, 2) 25 deg C, 17 h

2: 80 percent / piperidine / dimethylformamide / 17 h / 0 °C

With piperidine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86596-0

Reference yield:

: 134558-28-4
N-[(9H-fluoren-9-ylmethyloxy)-carbonyl]-α-methyl-DL-tryptophan

: 144876-63-1
phenylmethyl -<2-<<2-amino-3-(1H-indol-3-yl)-2-methyl-1-oxopropyl>amino>-1-phenylethyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide / 1) THF, EtOAc, 25 deg C, 2 h, 2) 25 deg C, 17 h

2: 80 percent / piperidine / dimethylformamide / 17 h / 0 °C

With piperidine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86596-0