1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

Base Information

Chemical Name:1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane
CAS No.:86525-71-5
Molecular Formula:C₁₁H₁₆O₃S
Molecular Weight:228.312
Hs Code.:

Synonyms:1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

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Chemical Property of 1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

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Technology Process of 1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

There total 1 articles about 1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 29421-92-9
4-bromo-2-methylthiophene

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 86525-71-5
1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

Guidance literature:: With sodium; potassium iodide; copper(II) oxide; at 90 ℃; for 36h;

Reference yield:

: 86525-71-5
1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

: Toluene-4-sulfonic acid 1-hydroxymethyl-2-(5-methyl-thiophen-3-yloxy)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 80percent AcOH / 0.5 h / 60 - 70 °C

2: pyridine / 24 h

With acetic acid; In pyridine;

Reference yield:

: 86525-71-5
1-(5-methyl-3-thienyloxy)-2,3-O-isopropylidene propane

: Toluene-4-sulfonic acid 2-hydroxy-3-(5-methyl-thiophen-3-yloxy)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 80percent AcOH / 0.5 h / 60 - 70 °C

2: pyridine / 24 h

With acetic acid; In pyridine;