trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

Base Information

Chemical Name:trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride
CAS No.:97168-74-6
Molecular Formula:C₁₁H₁₅NO₂*ClH
Molecular Weight:229.707
Hs Code.:

Synonyms:trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

Chemical Property:

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Technology Process of trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

There total 7 articles about trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 97133-73-8
trans-2-azido-trans-5-phenoxycyclopentanol

: 97168-74-6
trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 16h; under 2844.3 Torr;
DOI:10.1021/jo00217a017

Reference yield:

: 3212-60-0,6426-28-4,62894-08-0,109431-72-3
cyclopent-2-enol

: 97168-74-6
trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / vanadyl acetylacetonate, tert-butyl hydroperoxide / benzene / 1.) 80 deg C, 15 min, 2.) 40 deg C, 5 h

2: 79.5 percent / triphenylphosphine, isopropyl azocarboxylate / tetrahydrofuran / 24 h / Ambient temperature

3: 87 percent / sodium azide, ammonium chloride / ethanol; H₂O / 16 h / Heating

4: 67 percent / hydrogen, hydrochloric acid / 5percent Pd/C / ethanol / 16 h / 2844.3 Torr

With hydrogenchloride; tert.-butylhydroperoxide; sodium azide; di-isopropyl azodicarboxylate; vanadyl acetylacetonate; ammonium chloride; hydrogen; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; benzene;
DOI:10.1021/jo00217a017

Reference yield:

: 25484-62-2,29782-88-5,765-54-8,25516-47-6,34310-95-7,120577-03-9,139015-06-8
cis-6-oxabicyclo<3.1.0>cyclohexan-2-ol

: 97168-74-6
trans-2-amino-trans-5-phenoxycyclopentanol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 79.5 percent / triphenylphosphine, isopropyl azocarboxylate / tetrahydrofuran / 24 h / Ambient temperature

2: 87 percent / sodium azide, ammonium chloride / ethanol; H₂O / 16 h / Heating

3: 67 percent / hydrogen, hydrochloric acid / 5percent Pd/C / ethanol / 16 h / 2844.3 Torr

With hydrogenchloride; sodium azide; di-isopropyl azodicarboxylate; ammonium chloride; hydrogen; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo00217a017