methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate
CAS No.:1027548-99-7
Molecular Formula:C₂₆H₃₂N₂O₄
Molecular Weight:436.551
Hs Code.:

Synonyms:methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

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Chemical Property of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

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Technology Process of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

There total 5 articles about methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026685-78-8
4-[3-Acetoxymethyl-6-(2-ethyl-butylcarbamoyl)-indol-1-ylmethyl]-3-methoxy-benzoic acid methyl ester

: 1027548-99-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 18h; under 2585.7 Torr;
DOI:10.1021/jm00055a011

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 1027548-99-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

2: NaBH₄ / ethanol / 0.02 h / Heating

3: Et₃N / CH₂Cl₂ / 18 h / Ambient temperature

4: H₂ / 5percent Pd/C / ethyl acetate / 18 h / 2585.7 Torr

With sodium tetrahydroborate; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00055a011

Reference yield:

: 145889-35-6
6-<(2-ethylbutyl)carbamoyl>-3-formylindole

: 1027548-99-7
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>-3-methylindol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

2: NaBH₄ / ethanol / 0.02 h / Heating

3: Et₃N / CH₂Cl₂ / 18 h / Ambient temperature

4: H₂ / 5percent Pd/C / ethyl acetate / 18 h / 2585.7 Torr

With sodium tetrahydroborate; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00055a011