ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

Base Information

Chemical Name:ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate
CAS No.:1613269-84-3
Molecular Formula:C₁₇H₃₂N₂O₄
Molecular Weight:328.452
Hs Code.:

Synonyms:ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

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Chemical Property of ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

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Technology Process of ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

There total 2 articles about ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 39684-80-5
2-(tert-butoxycarbonylamino)ethyl bromide

: 76308-26-4
ethyl 2-((1r,4r)-4-aminocyclohexyl)acetate hydrochloride

: 1613269-84-3
ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

Guidance literature:: ethyl 2-((1r,4r)-4-aminocyclohexyl)acetate hydrochloride; With potassium carbonate; In dichloromethane; water; at 20 ℃; for 1h; Inert atmosphere;

2-(tert-butoxycarbonylamino)ethyl bromide; With N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water; for 18h; Reflux; Inert atmosphere;
DOI:10.1021/acs.jmedchem.9b00911

Reference yield:

: 1613269-84-3
ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

: 1613269-85-4
ethyl 2-[4-[2-(tert-butoxycarbonylamino)ethylamino]cyclohexyl]acetate

Guidance literature:: With methanol; sodium tetrahydroborate; at -78 ℃; for 1.25h;

Reference yield: 82.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1613269-84-3
ethyl 2-(trans-4-((2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

: 1613269-62-7
ethyl 2-(trans-4-((tert-butoxycarbonyl)(2-((tert-butoxycarbonyl)amino)ethyl)amino)cyclohexyl)acetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 16h; Reflux; Inert atmosphere;
DOI:10.1021/acs.jmedchem.9b00911