(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

Base Information

Chemical Name:(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine
CAS No.:1055874-41-3
Molecular Formula:C₂₂H₂₆N₂O₂
Molecular Weight:350.461
Hs Code.:

Synonyms:(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

Suppliers and Price of (3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

There total 1 articles about (3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 20989-17-7
(2S)-2-phenylglycinol

: 107-02-8,25068-14-8
acrolein

: 1055874-41-3
(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

Guidance literature:: In chloroform; at 20 ℃; for 0.0833333h;
DOI:10.1055/s-0033-1340859

Reference yield:

: 1055874-41-3
(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

: C₂₂H₃₀N₂O₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1055/s-0033-1340859

Reference yield:

: 1055874-41-3
(3S,9S)-3,9-diphenyloctahydro-5H,11H-bis[1,3]oxazolo[3,2-a:3',2'-e][1,5]diazocine

: C₃₆H₃₆Br₂N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

2: dmap; pyridine / 6 h / 80 °C / Inert atmosphere

With pyridine; dmap; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1055/s-0033-1340859