C₁₄H₁₆BrNO₃

Base Information

Chemical Name:C₁₄H₁₆BrNO₃
CAS No.:1311401-90-7
Molecular Formula:C₁₄H₁₆BrNO₃
Molecular Weight:326.19
Hs Code.:

C<sub>14</sub>H<sub>16</sub>BrNO<sub>3</sub>

Synonyms:C₁₄H₁₆BrNO₃

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Chemical Property of C₁₄H₁₆BrNO₃

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Technology Process of C₁₄H₁₆BrNO₃

There total 7 articles about C₁₄H₁₆BrNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31558-41-5
4-bromo-2,5-dimethoxybenzaldehyde

: 1311401-90-7
C₁₄H₁₆BrNO₃

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hypochlorite; disodium hydrogenphosphate; dihydrogen peroxide / water; acetonitrile / 20 °C / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Inert atmosphere

3: sodium hydroxide / dichloromethane; water / 2 h / Inert atmosphere

4: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 18 h / Inert atmosphere

5: boron trichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

6: toluene-4-sulfonic acid / toluene / 110 °C / Inert atmosphere

With sodium hypochlorite; disodium hydrogenphosphate; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; dihydrogen peroxide; boron trichloride; toluene-4-sulfonic acid; N,N-dimethyl-formamide; sodium hydroxide; In dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja204040k

Reference yield:

: C₁₅H₁₈BrNO₃

: 1311401-90-7
C₁₄H₁₆BrNO₃

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1021/ja204040k

Reference yield:

: C₉H₈BrClO₃

: 1311401-90-7
C₁₄H₁₆BrNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / dichloromethane; water / 2 h / Inert atmosphere

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 18 h / Inert atmosphere

3: boron trichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

4: toluene-4-sulfonic acid / toluene / 110 °C / Inert atmosphere

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; boron trichloride; toluene-4-sulfonic acid; sodium hydroxide; In dichloromethane; water; toluene;
DOI:10.1021/ja204040k