disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

Base Information

Chemical Name:disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane
CAS No.:107271-59-0
Molecular Formula:C₃₆H₅₂O₂*2Na
Molecular Weight:562.787
Hs Code.:

Synonyms:disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

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Chemical Property of disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

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Technology Process of disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

There total 4 articles about disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 107271-45-4
1,3-bis(3,5-di-tert-butyl-4-oxocyclohexa-1,5-dienylidene)-2,2,4,4-tetramethylcyclobutane

: 107271-59-0
disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

Guidance literature:: With sodium; In tetrahydrofuran; for 15h; Heating;
DOI:10.1021/jo00387a007

Reference yield:

: 10181-56-3
2,2,4,4-tetramethylcyclobutane-1,3-dithione

: 107271-59-0
disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / CCl₄ / 240 h / Ambient temperature

2: 55 percent / Na / tetrahydrofuran / 15 h / Heating

With sodium; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jo00387a007

Reference yield:

: 955-02-2
2,6-di-tert-butyl-4-diazo-2,5-cyclohexadien-1-one

: 107271-59-0
disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / CCl₄ / 240 h / Ambient temperature

2: 55 percent / Na / tetrahydrofuran / 15 h / Heating

With sodium; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jo00387a007