N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

Base Information

• Chemical Name: N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine
• CAS No.: 1022160-15-1
• Molecular Formula: C₄₁H₄₇N₃O₈
• Molecular Weight: 709.839

Synonyms:N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

Chemical Property of N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

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Technology Process of N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

There total 1 articles about N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate (1022160-14-0) → N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine (1022160-15-1)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 95.0%

N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine (1022160-15-1) + glycine ethyl ester hydrochloride (5680-79-5,883886-67-7) → methyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-16-2)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 95.0%

N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine (1022160-15-1) + glycine tert-butyl ester hydrochloride (27532-96-3) → tert-butyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-19-5)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

upstream raw materials:

methyl N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithinate

Downstream raw materials:

methyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

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