C₅₆H₉₄O₁₁Si

Base Information

Chemical Name:C₅₆H₉₄O₁₁Si
CAS No.:943898-09-7
Molecular Formula:C₅₆H₉₄O₁₁Si
Molecular Weight:971.441
Hs Code.:

C<sub>56</sub>H<sub>94</sub>O<sub>11</sub>Si

Synonyms:C₅₆H₉₄O₁₁Si

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Chemical Property of C₅₆H₉₄O₁₁Si

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Technology Process of C₅₆H₉₄O₁₁Si

There total 17 articles about C₅₆H₉₄O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₅₂H₈₆O₉Si

: 107-30-2
chloromethyl methyl ether

: 943898-09-7
C₅₆H₉₄O₁₁Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; Heating;
DOI:10.1021/ol070517g

Reference yield:

: 902132-11-0
(3R,4S)-3-(4-methoxybenzyloxy)-4-methyl-5-hexenal

: 943898-09-7
C₅₆H₉₄O₁₁Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3.19 g / CH₂Cl₂ / 12 h / 20 °C

2.1: 69 percent / oxygen; copper(II) acetate monohydrate / PdCl₂ / N,N-dimethyl-acetamide; H₂O / 12 h / 20 °C

3.1: ethyldiisopropylamine; dibutylboron triflate / CH₂Cl₂; diethyl ether / cooling

3.2: CH₂Cl₂; diethyl ether / cooling

3.3: 85 percent / aq. H₂O₂ / methanol; aq. phosphate buffer / pH 7

4.1: Et₂BOMe / tetrahydrofuran; methanol / cooling

4.2: 76 percent / NaBH₄ / methanol; tetrahydrofuran / cooling

5.1: 78 percent / ethyldiisopropyl amine / CHCl₃ / Heating

With di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; oxygen; copper diacetate; N-ethyl-N,N-diisopropylamine; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl acetamide; water; 1.1: Wittig reaction / 2.1: Wacker reaction / 3.2: Evans aldol reaction;
DOI:10.1021/ol070517g

Reference yield:

: 943897-88-9
C₂₀H₂₈O₄

: 943898-09-7
C₅₆H₉₄O₁₁Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 69 percent / oxygen; copper(II) acetate monohydrate / PdCl₂ / N,N-dimethyl-acetamide; H₂O / 12 h / 20 °C

2.1: ethyldiisopropylamine; dibutylboron triflate / CH₂Cl₂; diethyl ether / cooling

2.2: CH₂Cl₂; diethyl ether / cooling

2.3: 85 percent / aq. H₂O₂ / methanol; aq. phosphate buffer / pH 7

3.1: Et₂BOMe / tetrahydrofuran; methanol / cooling

3.2: 76 percent / NaBH₄ / methanol; tetrahydrofuran / cooling

4.1: 78 percent / ethyldiisopropyl amine / CHCl₃ / Heating

With di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; oxygen; copper diacetate; N-ethyl-N,N-diisopropylamine; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl acetamide; water; 1.1: Wacker reaction / 2.2: Evans aldol reaction;
DOI:10.1021/ol070517g