(R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate

Base Information

• Chemical Name: (R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate
• CAS No.: 1032077-69-2
• Molecular Formula: C₁₉H₃₀N₄O₃
• Molecular Weight: 362.472

Synonyms:(R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate

Chemical Property of (R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate

Chemical Property:

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Technology Process of (R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate

There total 1 articles about (R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

methyl 2-(4-acetylphenyl)-2-bromoacetate (1032077-66-9) + 1,4,7,10-tetraazacyclododecan (294-90-6) → (R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate (1032077-69-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 10h;

Reference yield: 83.0%

bromoacetic acid tert-butyl ester (5292-43-3) + (R/S)-methyl 2-[1-(1,4,7,10-tetraazacyclododecane)]-2-(4-acetylphenyl)acetate (1032077-69-2) → (R/S)-methyl 2-[1-(1,4,7,10-tetraazacydodecane)-4,7,10-tris(tert-butylacetate)]-2-(4-acetyl-phenyl)acetate (1032077-72-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4.5h;

upstream raw materials:

methyl 2-(4-acetylphenyl)-2-bromoacetate

1,4,7,10-tetraazacyclododecan

Downstream raw materials:

(R/S)-methyl 2-[1-(1,4,7,10-tetraazacydodecane)-4,7,10-tris(tert-butylacetate)]-2-(4-acetyl-phenyl)acetate

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