3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester

Base Information

• Chemical Name: 3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester
• CAS No.: 287408-51-9
• Molecular Formula: C₃₈H₄₈N₂O₁₀S₄
• Molecular Weight: 821.071

Synonyms:3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester

Chemical Property of 3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester

There total 2 articles about 3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

3,3'-dithiobis[N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester (287408-50-8) + allyl bromide (106-95-6) → 3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester (287408-51-9)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃;

Reference yield:

→ 3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester (287408-51-9)

Guidance literature:

Reference yield: 79.0%

3,3'-dithiobis[N-allyl-N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester (287408-51-9) + (E)-tert-butyl 4-bromobut-2-enoate (86606-04-4) → 18-(tert-butyl)-9,14-dimethyl(5E,9S,14S,17E)-8,15-bis{[4-(2-butynyloxy)phenyl]-sulfonyl}-2,2,10,10,13,13-hexamethyl-4-oxo-3-oxa-11,12-dithia-8,15-diazaoctadeca-5,17-diene-9,14,18-tricarboxylate

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide);

upstream raw materials:

3,3'-dithiobis[N-[[4-(2-butynyloxy)phenyl]sulfonyl]-D-valine] dimethyl ester

allyl bromide

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